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Beilstein J. Org. Chem. 2018, 14, 2289–2294, doi:10.3762/bjoc.14.203
Graphical Abstract
Figure 1: Tautomerism in iodine-based group-transfer reagents probed by 17O NMR spectroscopy (A) and key stru...
Figure 2: Assignment of acyclic (b) and cyclic (a) structures to 5 and 6, respectively, based on computed iso...
Figure 3: Protonation of 4a with trifluoroacetic acid (5 equiv) affords 4c, followed by 17O NMR spectroscopy.
Beilstein J. Org. Chem. 2014, 10, 1–6, doi:10.3762/bjoc.10.1
Figure 1: Electrophilic trifluoromethylating agents 1 and 2.
Scheme 1: Synthesis of 5-nitro-1-(trifluoromethyl)-3H-1λ3,2-benziodaoxol-3-one (3).
Figure 2: UV–vis spectra of reagents 2 (green) and 3 (blue) in DMSO/H2O 1:1.
Figure 3: ORTEP representation of X-ray structures 6 and 3. Thermal ellipsoids set to 30% probability. Hydrog...
Figure 4: DSC traces obtained for 2 (green) and 3 (blue).
Figure 5: Cyclic voltammetry of 3 (1 mM, black) and of a mixture of 3 (1 mM) and methyl 2-iodo-5-nitrobenzoat...
Figure 6: Sample kinetic traces for the decomposition of 2 (green) and 3 (blue) to 4 and 5, respectively, upo...